- Research Article
- 10.1088/1742-6596/3194/1/012013
Electron beam treatment of complex titanium-copper oxide films for biomedical applications
- Mar 01, 2026
- Journal of Physics: Conference Series
- M P Nikolova + 5 more +5
Abstract This work investigates the impact of electron beam treatment (EBT) on Ti–Cu oxide coatings deposited on Ti6Al4V via reactive DC magnetron sputtering (MS). The as-deposited films, mainly anatase TiO 2 with minor Cu phases, were post-treated using beam currents of 1 mA and 2 mA. Surface and structural analyses (SEM/EDS, XRD) revealed densification and partial anatase-to-rutile transformation at higher energy input, accompanied by grain coarsening. Mechanical tests revealed a slight decrease in hardness but a significant improvement in adhesion, with critical loads exceeding 30 N following post-EBT treatment. Electrochemical studies in simulated body fluid indicated a strong reduction in corrosion current density for all coatings, with protection efficiencies above 98% at low beam energy. Additionally, EBT reduced copper ion release during immersion, linked to surface densification and phase evolution. The combined MS deposition + EBT treatment enhances adhesion, corrosion resistance, and ion release control, making these coatings promising for biomedical implant applications.
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