- Research Article
- 10.32684/2412-5288-2025-2-27-43-49
ASSESSMENT OF SUITABILITY OF VERIFICATION / VALIDATION OF CALIBRATION METHODOLOGY
- Jan 01, 2025
- Key title Zbìrnik naukovih pracʹ Odesʹkoï deržavnoï akademìï tehnìčnogo regulûvannâ ta âkostì
- А А Haber + 4 more +4
The article considers the issue of ensuring the reliability of measurements in testing and calibration laboratories by implementing a structured methodology for assessing the suitability of methods (methodologies) based on verification and validation procedures. The sequence of assessment stages is presented - from planning, selection of the methodology and analysis of calibration requirements to conducting experimental studies, determining accuracy parameters, estimating uncertainty and making a decision on the suitability of the method. The criteria used in the analysis of calibration results are described in detail, in particular, determining confidence intervals, estimating errors, checking the acceptability of results according to the En criterion, as well as the procedure for documenting the procedure in accordance with the requirements of regulatory and technical documents. The work systematizes the factors that affect the metrological quality of measurements, including the choice of measuring instruments, the qualifications of performers, the conditions for conducting measurements and the correctness of the application of methods. The proposed assessment system allows you to reduce the probability of errors, increase the accuracy and reproducibility of results, as well as ensure compliance of measurement processes with the requirements of DSTU EN ISO/IEC 17025:2019 and other regulatory documents. The results obtained can be used by laboratories to improve their internal quality system, increase the reliability of test equipment and optimize calibration processes.
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