A quick and low-cost smartphone photogrammetry method for obtaining 3D particle size and shape

Three-dimensional particle shape characterizations from half particle geometries

Experimental investigation of segregation in a rotating drum with non-spherical particles

Samples of soils collected by the Apollo 11 mission (10084,2036) and the Apollo 14 mission (14163,940) were obtained from the NASA Curation and Analysis Planning Team for Extraterrestrial Materials (CAPTEM) program. The particle size, shape, and internal porosity were characterized in three dimensions (3D) using a combination of X-ray computed tomography (XCT) and mathematical analysis, with various size and shape parameters measured and calculated for each particle. High-resolution scanning electron microscopy (SEM) was used to image the particles that were too small for the two XCT instruments used. Similar characterization was carried out on samples of JSC-1A lunar soil simulant, updating a previous analysis. Approximately 14,000 lunar regolith particles and 128,000 JSC1-A particles, covering a wide range of size and shape, were characterized for this paper and the results stored in a publicly accessible database. This large number of particles enabled, for the first time, statistically valid particle shape distributions to be generated. The 3D shape distributions of the two regoliths and JSC-1A were quantitatively compared and it was found that the way particle shape and porosity depends on particle size was different between regolith and simulant. The measured size distribution of particles in the lunar soils was applied to estimate the relative contributions of different sizes to the ensemble average particle single scattering albedo and phase function. By linking our particle counts to published sieve weight fractions for the lunar samples, we find that ∼80% of the total cross-section area is contributed by particles <20 μm diameter and ∼ 50% by particles <8 μm diameter. The orientation-averaged two-dimensional projected areas of the actual regolith particles were computed so that this estimate was also based on real particle shapes. Such small sizes dominating the total cross-section area suggest that calculations of the elements of the scattering matrix for individual particles may be possible with modest computing capabilities leading to the development of improved models for the quantitative interpretation of remote sensing spectrophotometry and polarimetry. This 3D characterization and database will enable other computational work to be done with real lunar regolith particle shapes, including discrete element method mechanical modeling, packing simulations, further light scattering calculations, dust contamination modeling, and modeling of lunar rover interactions with collected and packed regolith particles.

Performance study of SBS/CRMA with different composite crumb rubber particle size ratios

It's usually known that the particle size and particle shape are two irrelevant concepts. But our research shows that the token of particle size is not only related to particle shape, but also related to particle measurement methods. This paper takes sheetlike graphite micropowder for example and gets the function relation between particle shape factor and particle size by analyzing the particle distribution data between laser diffraction and sedimentation. This research provides a new approach for the study of particle shape.

A study has been made of the effects of particle size and particle shape on the shear and tensile properties of batches of dried procaine penicillin powders whose particle shapes were varied by crystallization from different solvents. The following correlations have been established between the mechanical parameters of the powders and their particle size and shape. log C/T = 1·706 − 0·213 log (V/S) — 1·36 αs.v.a.; (n − 1) = 1·329 + 0·0083 (V/S) − 0·128 αs.v.a.; tan Δ= 0·812 + 0·0057 (V/S) + 0·025 αs.v.a.; FF = 6·52 + 0·434 (V/S) − 0·528 αs.v.a. The findings are discussed in relation to the design of filling equipment for unit doses of penicillin.

Our aim was to analyse the influence of the size, shape and number of particles on the pathogenesis of osteolysis. We obtained peri-implant tissues from 18 patients having revision surgery for aseptically loosened Freeman total knee replacements (10), Charnley total hip replacements (3) and Imperial College/London Hospital double-cup surface hip replacements (5). The size and shape of the polyethylene particles were characterised using SEM and their concentration was calculated. The results were analysed with reference to the presence of radiological osteolysis. The concentration of polyethylene particles in 6 areas with osteolysis was significantly higher than that in 12 areas without osteolysis. There were no significant differences between the size and shape of the particles in these two groups. We conclude that the most critical factor in the pathogenesis of osteolysis is the concentration of polyethylene particles accumulated in the tissue.

High-pressure uniaxial compression tests were conducted under strain-controlled conditions using spherical glass beads. The study focused on investigating the compression behavior and particle fragmentation phenomena, particularly observing changes in particle size and shape resulting from fragmentation. The examination of particle shape, specifically sphericity and roundness, was emphasized. The samples comprised glass beads with uniform particle size and shape initially. It was observed that pressures exceeding 20MPa triggered particle fragmentation, leading to significant compression behavior. Notably, a softening phenomenon characterized by rapid fluctuations in compressive stress, despite a monotonic increase in strain, was observed during fragmentation. This phenomenon indicates the particles' catastrophic failure, unable to withstand the contact forces they previously sustained. Observations of particle shape revealed trends toward asymptotic distributions in cumulative curves for particle size, sphericity, and roundness. Moreover, changes in the cumulative curve of roundness were more pronounced compared to particle size and sphericity.

Synthesis of zeolitic imidazolate framework-8 particles of controlled sizes, shapes, and gate adsorption characteristics using a central collision-type microreactor

Macroscopic mechanical properties of granular materials are closely related to particle morphology. For practical reasons, the morphological features are commonly examined from projected two-dimensional (2D) images of the three-dimensional (3D) particles. This brings forward the need for quantifying the correlations between the 2D and 3D particle descriptors. This paper addresses these correlations for irregular granular particles. Three-dimensional images of sand particles were acquired through microfocus X-ray computed tomography, based on which 3D surfaces of the particles were reconstructed using spherical harmonic analyses. The 3D particle size and shape descriptors were subsequently evaluated. All-around projection and random projection of the particles onto 2D planes were undertaken numerically to obtain the projected 2D images and thus the corresponding 2D size and shape descriptors. The results indicate that there are close correlations between 3D and 2D size descriptors averaged from the all-around projections. 2D and 3D shape descriptors can be approximately fitted with a linear relationship. The mean value of 2D descriptors of the tested sands obtained from a series of independent random-projection tests is essentially identical to that from the all-around projections; except that the data from the random-projection tests show a larger scatter. In light of the relationships among the descriptors, a novel and promising approach to predict the cumulative distribution of 3D descriptors from that of 2D descriptors evaluated from a random-projection test is proposed.

Influences of ball-milled limestone particle sizes and shapes on asphalt mastic stress relaxation behavior

SUMMARYResearch backgroundWholewheat flour is a very good source of nutritional compounds and functional ingredients for human diet. However, it causes negative effect on bread quality. Different milling techniques can be used to obtain wholewheat flour, minimizing the negative effect of both bran and germ on bread quality. The aim of this work is to study the effect of particle size and shape of wholegrain flour on the interaction among the different components, water distribution, dough rheology and bread volume.Experimental approachWholewheat flour of three varieties (Klein Rayo, Fuste and INTA 815) was obtained in cyclonic, hammer and roller mills. The characteristics of wholewheat flour were explored, and the water distribution and rheological properties of dough were determined by thermogravimetric analysis and Mixolab test, respectively. Finally, microscale bread was prepared.Results and conclusionsThe amount of water-soluble pentosans, damaged starch and wet gluten was affected by the milling procedure. Regarding dough rheological properties, wholewheat flour obtained in hammer mill had the lowest water absorption capacity and the highest developing time. This result could be mainly attributed to particle shape in these samples with large amount of endosperm attached to the bran, hindering protein unfolding. Thermogravimetric analysis showed that both fine and large bran particle size seem to have the same effect on water properties in wholewheat dough during heating. Bread made with Klein Rayo variety had the highest specific volume, indicating that wheat with high protein content and breadmaking quality is needed to make wholewheat bread. The results of this work showed that particle shape, rather than particle size, affected the quality of wholewheat flour for breadmaking.Novelty and scientific contributionThe effect of milling type and particle shape of the wholewheat flour had a greater effect than the wheat variety. Thus, the wholegrain milling process should be carefully selected taking to account the shape of the produced particle. This may open new opportunities for developing wholewheat bread with better acceptance by consumers.

ABSTRACTSmall particles are of interest for magnetic study due to their range of magnetic properties with particle size and unusual magnetic properties. In this study we produced graphite encapsulated magnetic cobalt particles and measured their structural and magnetic properties both before and after annealing at 550° C for 6 hours. No large change in the structural properties (particle size, shape, and lattice parameter) was observed as a result of the annealing. There were, however, significant changes in the magnetic properties. The coercivity was found to decrease at all temperatures, especially at temperatures below 100° K. The possible reasons for this reduction in coercivity are examined, with the change in the shape of the particles appearing most likely.

The majority of cells and microorganisms have a nonspherical shape and complex structure that challenge the interpretation of their spectral features. To address this issue, two approximations to the core-shell Mie theory were proposed. These included the approximation of light extinction by an ellipsoid with representation of the extinction by an equivalent sphere and representation of the extinction by a population of ellipsoidal particles with those of two weighted particle orientations. These hypotheses were first tested through numerical interpretation of the theoretical extinction spectra of prolate nucleated ellipsoids mimicking biological cells generated with anomalous diffraction approximation used as a reference method. Theoretical cases of fixed and random particle orientations demonstrated excellent capabilities of the proposed approach to retrieve the size, shape, and composition parameters of the model particles. Second, the UV-visible spectra of Leishmania species, promastigotes, elongated cells with prominent nuclei, were interpreted. The retrieved estimates of the protozoa size, shape, nucleus size, and nucleotide composition were in agreement with the corresponding microscopy estimates and literature values. Both theoretical tests and experimental results illustrated that the proposed approach can be successfully applied to estimate the structural and compositional parameters of cells from spectroscopic measurements.

Background and purposeThe study evaluated the differences in leaf positioning deviations by the log files of three advanced accelerators with two delivery techniques, and established specific assessment parameters of leaf positioning deviations for different types of accelerators.MethodsA total of 420 treatment plans with 5 consecutive treatment log files were collected from the Trilogy, TrueBeam and Halcyon accelerators. Millennium MLC was equipped on the Trilogy and TrueBeam accelerators. A jawless design and dual-layer MLC were adopted on the Halcyon accelerator. 70 IMRT and 70 VMAT plans were selected randomly on each accelerator. The treatment sites of all plans included head and neck, chest, breast, pelvis and other sites. The parsing tasks for 2100 log files were proceeded by SunCheck software from Sun Nuclear Corporation. The maximum leaf root mean square (RMS) errors, 95th percentile errors and percentages of different leaf positioning errors were statistically analyzed. The correlations between these evaluation parameters and accelerator performance parameters (maximum leaf speed, mean leaf speed, gantry and arc angle) were analyzed.ResultsThe average maximum leaf RMS errors of the Trilogy in the IMRT and VMAT plans were 0.44 ± 0.09 mm and 0.79 ± 0.07 mm, respectively, which were higher than the TrueBeam's 0.03 ± 0.01 mm, 0.03 ± 0.01 mm and the Halcyon's 0.05 ± 0.01 mm, 0.07 ± 0.01 mm. Similar data results were shown in the 95th percentile error. The maximum leaf RMS errors were strongly correlated with the 95th percentile errors (Pearson index > 0.5). The leaf positioning deviations in VMAT were higher than those in IMRT for all accelerators. In TrueBeam and Halcyon, leaf position errors above 1 mm were not found in IMRT and VMAT plans. The main influencing factor of leaf positioning deviation was the leaf speed, which has no strong correlation with gantry and arc angles.ConclusionsCompared with the quality assurance guidelines, the MLC positioning deviations tolerances of the three accelerators should be tightened. For both IMRT and VMAT techniques, the 95th percentile error and the maximum RMS error are suggested to be tightened to 1.5 and 1 mm respectively for the Trilogy accelerator. In TrueBeam and Halcyon accelerators, the 95th percentile error and maximum RMS error of 1 and 0.5 mm, respectively, are considered appropriate.