Features of obtaining bentonite-based ceramic support using SLS 3D printing

Modeling and prediction of surface roughness and dimensional accuracy in SLS 3D printing of PVA/CB composite using the central composite design

To address the shortcomings of large porosity and insufficient mechanical properties of skeletonized Thermoplastic polyurethane (TPU) fabrications during the preparation of composite materials by selective laser sintering (SLS) technology. In this paper, SiO2@Si3N4ws‐GPTMS core‐shell structure filler was successfully prepared by first synthetically growing silicon dioxide (SiO2) nanospheres on the surface of silicon nitride whiskers (Si3N4ws) in situ by sol–gel method, and then modified with silane coupling agent Silane coupling agent (GPTMS). Then the filler was incorporated into the inner and outer surfaces of TPU skeletonized structural parts by vacuum dip coating using a water‐based polyurethane (PU) coating post‐treatment enhancement method, and the surface coating coating of TPU skeletonized structural parts was achieved by warming and curing. This composite filler coating structure greatly improved the mechanical properties of the SLS parts (tensile strength of 20.3 MPa and elongation at break of 338.9%, 163% higher tensile strength, 17.7% higher elongation at break, and 672% higher rebound dimension compared with the pure TPU sintered parts). In addition, the thermal stability of the SLS sintered parts was improved, which greatly enhanced the application of the sintered manufactured parts prepared by SLS technology in the field of rebound‐absorbing artificial wear.

Fabrication of porous polyvinyl alcohol scaffold for bone tissue engineering via selective laser sintering

PURPOSEOne of the most important factors in evaluating the quality of fixed dental prostheses (FDPs) is their gap. The purpose of this study was to compare the marginal and internal gap of two different metal-ceramic crowns, casting and selective laser sintering (SLS), before and after porcelain firing. Furthermore, this study evaluated whether metal-ceramic crowns made using the SLS have the same clinical acceptability as crowns made by the traditional casting.MATERIALS AND METHODSThe 10 study models were produced using stone. The 20 specimens were produced using the casting and the SLS methods; 10 samples were made in each group. After the core gap measurements, 10 metal-ceramic crowns in each group were finished using the conventional technique of firing porcelain. The gap of the metal-ceramic crowns was measured. The marginal and internal gaps were measured by two-dimensional and three-dimensional replica techniques, respectively. The Wilcoxon signed-rank test, the Wilcoxon rank-sum test and nonparametric ANCOVA were used for statistical analysis (α=.05).RESULTSIn both groups, the gap increased after completion of the metal-ceramic crown compared to the core. In all measured areas, the gap of the metal cores and metal-ceramic crowns produced by the SLS was greater than that of the metal cores and metal-ceramic crowns produced using the casting. Statistically significant differences were found between cast and SLS (metal cores and metal-ceramic crown).CONCLUSIONAlthough the gap of the FDPs produced by the SLS was greater than that of the FDPs produced by the conventional casting in all measured areas, none exceeded the clinically acceptable range.

Improving accuracy through shrinkage modelling by using Taguchi method in selective laser sintering

Synergistic application of twin-screw granulation and selective laser sintering 3D printing for the development of pharmaceutical dosage forms with enhanced dissolution rates and physical properties

Investigation into the processability, recyclability and crystalline structure of selective laser sintered Polyamide 6 in comparison with Polyamide 12

Metal-ceramic bond strength of a cobalt chromium alloy for dental prosthetic restorations with a porous structure using metal 3D printing

An increasing demand for additively manufactured polymer composites with optimized mechanical properties is manifesting in different industries such as aerospace, biomedical, and automotive. Laser sintering (LS) is an additive manufacturing method that has the potential to produce reinforced polymers, which can meet the stringent requirements of these industries. For the development of a commercially viable LS nylon-based composite material, previous research studies worldwide have focused on adding glass beads to the powder material with the goal to produce fully dense parts with properties more representative of injection molded (IM) thermoplastic composites. This led to the development of a commercially available glass bead-filled polyamide 12 (PA12) powder. Although this powder has been on the market for quite a while, an in-depth comparison of the mechanical behavior of laser sintered versus IM glass bead-filled PA12 is lacking. In this study, laser-sintered glass bead-filled PA12 samples were built in different orientations and compared to IM counterparts. After sample production, the mechanical performance of the produced LS and IM parts was tested and compared to evaluate the quasistatic and dynamic mechanical performance and failure mechanisms at different load levels. In addition, the glass bead-filled PA12 properties were also compared to those of standard (unfilled) LS PA12 to assess whether glass beads actually improve the mechanical performance and fatigue lifetime of the final LS samples, as suggested in literature. Results in this work present and explain the increased stiffness but decreased fatigue life of glass bead-filled polyamide parts made by LS and IM. This research can be regarded as a "benchmark" study, in which samples produced from commercially available, filled and unfilled, PA12 powder grades are compared for both LS and conventional production techniques.

Purpose – This work aims to investigate the direct production of electrical discharge machining (EDM) electrodes by means of the selective laser sintering (SLS) technique using a new non-conventional metal-matrix composite material (TiB2-CuNi). The influence and optimization of the main SLS parameters on the densification behavior and porosity is experimentally studied. EDM experiments are also performed to evaluate the electrodes performance. Design/methodology/approach – The new EDM electrode material used was a powder system composed of TiB2 and CuNi. Making use of a designed systematic experimental methodology, the effects of layer thickness, laser scan speed and scan line spacing were optimized, where aspects such as densification behavior, porosity and surface morphology of the samples were analyzed through microstructural and surface analysis. EDM experiments were conducted under three different regimes in order to observe the electrodes behavior and performance. The results were compared with copper powder electrodes manufactured by SLS and EDMachined under the same conditions. Findings – The experimental results showed that the direct SLS manufacturing of composite electrodes is feasible and promising. The laser scan speed has a high effect on the densification behavior of the samples, while the effect of scan line spacing on the porosity is more visible when the overlapping degree is considered. Surface morphology was not affected by the scan line spacing, whereas balling phenomenon was reported, regardless of the scan line spacing. The EDM results showed that the TiB2-CuNi electrodes had a much superior performance than the copper powder electrodes made by SLS, regardless of the EDM regime applied. Research limitations/implications – Generally, the machine tool itself promotes some restrictions to the SLS process optimization. It is normally attributed to the characteristics of the laser type and the amount of energy that can be delivered to the powder bed. The present investigation could not cover all the optimization potential involved with the studied material due to limitations of the SLS machine tool used. Originality/value – Significant results on the direct SLS manufacturing of a new non-conventional composite material, which has a great technological potential to be used as an EDM electrode material, are presented. Valuable guidelines are given in regard to the SLS optimization of TiB2-CuNi material and its performance as an EDM electrode. This work also provides a systematic methodology designed to be applied to the SLS process to produce EDM electrodes.

Mechanical properties of graded scaffolds developed by curve interference coupled with selective laser sintering.

Purpose – This work is focused on the investigation of direct production of electrical discharge machining (EDM) electrodes through the selective laser sintering (SLS) technique using a new metal-matrix composite material made of molybdenum and a copper-nickel alloy (Mo-CuNi). The influence and optimization of the main SLS parameters on the densification behavior and porosity is experimentally studied. Additionally, EDM experiments are performed to evaluate the electrodes performance under different machining conditions. The paper aims to discuss these issues. Design/methodology/approach – The new EDM electrode material used was a powder system composed of Mo and pre-alloyed CuNi. A systematic experimental methodology was designed to evaluate the effects of layer thickness, laser scan speed and hatch distance. The densification behavior, porosity and surface morphology of the samples were analyzed through microstructural and surface analysis. EDM experiments were conducted under three different regimes in order to observe the electrodes behavior and performance. The results were compared with copper powder electrodes manufactured by SLS and solid copper electrodes EDMachined under the same conditions. Findings – The experimental results showed that the direct SLS manufacturing of composite electrodes is feasible and an adequate combination of parameters can produce parts with good quality. The laser scan speed has a great effect on the densification behavior of the samples, while the effect of hatch distance on the porosity is more visible when the overlapping degree is considered. The overlapping also had a significant effect on the surface morphology. The EDM results showed that the Mo-CuNi electrodes had superior performance to the copper powder electrodes made by SLS for all the EDM regimes applied, but inferior to those achieved with solid copper electrodes. Originality/value – Significant results on the direct SLS manufacturing of a new material which has a great technological potential to be used as an EDM electrode material are presented. Valuable guidelines are given in regard to the SLS optimization of Mo-CuNi material and its performance as an EDM electrode. This work also provides a systematic methodology designed to be applied to the SLS process to produce EDM electrodes.

Selective Laser Sintering (SLS) is an Additive Manufacturing (AM) technology that is receiving considerable attention in the scientific and industrial communities due to its great ability to efficiently produce functional and complex parts. The present work aims to fabricate a real prototype via SLS, such as a hose reel for industrial applications, using polyamide 11 (PA11) as a starting material. Characterization of the PA11 powder properties was first carried out from a thermal and morphological viewpoint to determine the powder's thermal stability by TGA, the sintering window and degree of crystallinity by DSC, and the microstructure by SEM, PSD, and XRD analyses. The results revealed that PA11 has a 45-micron average particle size, circularity close to 1, and a Hausner ratio of 1.17. Together, these parameters ensure that PA11 powder flows smoothly, packs uniformly, and forms dense and defect-free layers during the SLS process, directly contributing to high part quality, dimensional precision, and stable process performance. The printability of the PA11 was optimized for the realization of 3D-printed parts for industrial applications. Finally, the quality of the printed samples and the mechanical and thermal performance were investigated. Several PA11-based parts were fabricated via SLS, showing a high level of complexity and definition, ideal for industrial applications, as confirmed by the predominantly green areas of the colored maps of X-CT. A complete prototypal case for a hose reel was assembled by using the parts realized, and it was chosen as a technological demonstrator to verify the feasibility of PA11 powder in the production of industrial professional components.

Design of SLS 3D-printed pediatric combination printlets of lamivudine and tenofovir disoproxil fumarate by understanding the impact of formulation and process variables on flow, spectral, thermal and performance characteristics.

Polyetheretherketone (PEEK) is a bioinert thermoplastic that has been investigated for its potential use in craniofacial reconstruction; however, its use in clinical practice is limited by a poor integration with adjacent bone upon implantation. To improve the bone-implant interface, two strategies have been employed: to modify its surface or to impregnate PEEK with bioactive materials. This study attempts to combine and improve upon the two approaches by modifying the internal structure into a trabecular network and to impregnate PEEK with mesenchymal stem cells. Furthermore, we compare the newly designed PEEK scaffolds' interactions with both bone-derived (BMSC) and adipose (ADSC) stem cells. Customized PEEK scaffolds were designed to incorporate a trabecular microstructure using a computer-aided design program and then printed via selective laser sintering (SLS), a 3D-printing process with exceptional accuracy. The scaffold structure was evaluated using microCT. Scanning electron microscopy (SEM) was used to evaluate scaffold morphology with and without mesenchymal stem cells (MSCs). Adipose and bone marrow mesenchymal cells were isolated from rats and cultured on scaffolds. Cell proliferation and differentiation were assessed using alamarBlue and alkaline phosphatase assays, respectively. Cell morphology after one week of co-culturing cells with PEEK scaffolds was evaluated using SEM. SLS 3D printing fabricated scaffolds with a porosity of 36.38% ± 6.66 and density of 1.309 g/cm(2). Cell morphology resembled viable fibroblasts attaching to the surface and micropores of the scaffold. PEEK scaffolds maintained the viability of both ADSCs and BMSCs; however, ADSCs demonstrated higher osteodifferentiation than BMSCs (p < 0.05). This study demonstrates for the first time that SLS 3D printing can be used to fabricate customized porous PEEK scaffolds that maintain the viability of adipose and bone marrow-derived MSCs and induce the osteodifferentiation of the adipose-derived MSCs. The combination of 3D printed PEEK scaffolds with MSCs could overcome some of the limitations using PEEK biopolymers for load-bearing bone regeneration in craniofacial reconstruction.