- Research Article
- 10.2334/josnusd.25-0397
Shear bond strength of resin luting material to zirconia using a pre-sintered coating approach.
- Apr 16, 2026
- Journal of oral science
- Satomi Arai + 3 more +3
The effect of a feldspathic porcelain coating applied before or after zirconia sintering on the shear bond strength between a resin luting agent and zirconia was evaluated. Pre-sintered and fully sintered zirconia specimens were coated with feldspathic porcelain and divided into three surface treatment groups: no treatment, airborne-particle abrasion, and hydrofluoric acid etching. The specimens were bonded using a dual-polymerizing resin luting agent and subjected to 0 or 5,000 thermocycles. The shear bond strength was measured. The fracture modes were analyzed microscopically. The surface morphology and composition were examined by scanning electron microscopy (SEM) and X-ray diffraction. Before thermocycling, both airborne-particle abrasion and hydrofluoric acid etching significantly increased the bond strength compared with no treatment. After thermocycling, airborne-particle abrasion maintained the highest bond durability, while hydrofluoric acid etching showed a marked decrease. SEM revealed that airborne-particle abrasion produced a rough surface favorable for micromechanical retention, whereas hydrofluoric acid etching resulted in smoother morphology. Airborne-particle abrasion effectively enhanced and preserved the bond strength between the resin luting agent and feldspathic porcelain-coated zirconia, regardless of the coating sequence. Hydrofluoric acid etching was ineffective after thermocycling, likely due to surface precipitation that occurred during firing.
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