ABSTRACTShort-duration archeological sites situated entirely within plateaus in the radiocarbon calibration curve pose unique challenges for our understanding of past processes at regional and global scales. This paper aims to overcome these limitations by leveraging the specific characteristics of two depositional contexts, the Early Neolithic Swifterbant Culture sites S3 and S4, located in the Dutch wetlands. These sites are of exceptional significance as they provide the earliest conclusive evidence of crop cultivation and animal husbandry outside the expansion of Linearbandkeramik (LBK) farmers in north-western Europe. Here, we present a customized approach that combines radiocarbon dating and Bayesian modeling, predicated on vertical sequences of short-lived plant remains. Our innovative approach enables us to determine, at a fine scale, the temporal position and duration of the prominent archeological contexts at S3 and S4, and explore the chronological relationship between the two sites. Through our analysis, we propose a new chronology for the onset of Neolithization in the Dutch wetlands.

ABSTRACTThe conquest of the Shang Dynasty at Anyang around 1046 BCE by the Zhou is one of the major events for not only Chinese Bronze Age but also early interaction between the pastoralist groups from the Eurasian Steppes and agriculture ones in the Central Plains of China. It is well-known from historical texts that the pre-Zhou people lived in the ancient Bin region (豳), the exact location of which is unclear, but most likely in the Jing River valley. At some point the leader Gugong Danfu (古公亶父) moved from Bin to the capital Qi (Zhouyuan), which preceded the Zhou invasion of Anyang. We have produced a new high resolution radiocarbon chronology for Zaolinhetan, a small settlement in the pre-Zhou heartland. This shows not only an exceptionally long chronological span for the site, but also a different phasing compared to the traditional pottery typology, which raises new questions regarding the regional variation of pottery typologies. Intriguingly, the analysis also reveals a rapid abandonment of Zaolinhetan around 1100 BCE, at the same time many larger sites, such as Zhouyuan, which later became the capital of the Western Zhou dynasty, were significantly expanding. We argue that the drastic decline of Zaolinhetan as revealed by the substantial number of radiocarbon dates and probably also the movement of pre-Zhou political center from Bin to Qin, was part of bigger picture that involved a range of social and environmental factors.

ABSTRACTOver the course of one year (2021), we monitored the carbon isotope composition of atmospheric CO2 at three locations in Croatia: the Adriatic port city of Rijeka (Cfa climate) and at two rural sites: Gornje Jelenje (Cfb climate) in the vicinity of a main road and clean-air site Parg (Dfb climate). Carbon isotope composition at all sites shows seasonal variation, ranging from –41.3 to 25.2‰ for Δ14C and from –13.1 to –11.3‰ for δ13C. Rijeka systematically has the lowest and Parg the highest Δ14C, and δ13C at the sites are not statistically different one from another. The Δ14C of leaves of deciduous trees reflect the trend of atmospheric Δ14C. Based on the assumption that the investigated area is under the influence of two main sources of CO2: fossil and natural (sea exchange, biosphere, and undisturbed – clean air atmospheric component) the approximate share of fossil CO2 in total atmospheric CO2 has been estimated for Rijeka (2.1 ± 1.3%) and Gornje Jelenje (1.0 ± 0.9%). Comparison of our results with the data from European CO2 sampling stations indicates strong influence of CO2 from sea and biosphere. Backward trajectories indicate a possibility of Δ14CCO2 contribution from distant EU nuclear power plants, but movement of air masses should be considered in more detail to confirm this.

ABSTRACTAs there exists a growing demand for chronological research and tracer applications using radiocarbon (14C) analyses of samples smaller than 100 μg C, a compact micro-specific hydrogen graphitization method has been developed at the Xi’an Accelerator Mass Spectrometry (AMS) Center. This article describes the performance of the system and the mass of carbon background produced during ultra-small sample preparation. Furthermore, we discuss the results of contamination corrections and perform 14C analyses on small samples with known age or reference values. The results reveal that our 14C analysis of ultra-small samples of 10–100 μg C can obtain accurate and reliable results, and the micro-scale 14C-AMS analysis technique meets our research objectives for dating and tracer applications.

ABSTRACTThe Laboratoire des Sciences du Climat et de l’Environnement (LSCE) has operated a radiocarbon dating laboratory for almost 70 years. It has evolved from a traditional ß-decay counting to an accelerator mass spectrometry facility. In 2015, the LSCE received a major upgrade with the installation of a MICADAS. This evolution required adjustments in sample preparation to match the new capability to date samples as small as a few tens of µgC. We summarize here the sample cleaning procedures and the chemical purification or extraction treatment that we apply to the samples. We also report values of blank and reference materials of different matrices that match the large diversity of samples handled at LSCE.

ABSTRACTNitra-Lupka is an important site from the Great Moravian period in Slovakia. A fortified hillfort which was supposed to be from this period, a battery of pottery kilns, and an Early Medieval cemetery were found on the site and researched during 1959–1975. Further, a few small-range excavations took place on the site at the beginning of the 21st century. At the same time, the dating of the hillfort to the Early Medieval period has begun to be questioned. There was also a problem with the localization of settlement that would belong to the battery of pottery kilns. The settlement was discovered recently in 2021 during development-led excavations at Nitra-Šindolka. It was found at the place of the construction of the ecoduct. Two ovens and four other features with numerous ceramics and other findings were discovered. Some of the bones (phalanges of cattle and goat/sheep) were dated by radiocarbon dating being the first 14C data obtained from this site and therefore of high importance for its precise dating.

ABSTRACTIn the absence of wood, bone, and other organics, one possible candidate for determining the age of a site is the radiocarbon (14C) dating of pottery. In central Europe during the Early Neolithic, pottery was ubiquitous and contained substantial quantities of organic temper. However, attempts at the direct dating of organic inclusions raises a lot of methodological issues, especially when several sources of carbon contribute to the resulting radiocarbon age. Hence an alternative approach to dating of the early pottery is necessary. Here, we present a novel method of bulk separation of organic content from the grass-tempered pottery from Santovka (Slovakia). The procedure is based on the consecutive application of three inorganic acids, dissolving clay, silica content, and low molecular or mobile fractions to separate organic inclusions added to the pottery matrix during the formation of vessels. Radiocarbon dates obtained with this method are coherent and produce the shortest time span compared to other pretreatment methods presented in this study. The paired dates of grass-tempered pots with the 14C age of lipids extracted from the same pots point to a difference of 400–600 14C yr, however they are in line with the site’s chronostratigraphic Bayesian model. Grass-tempered pottery from Santovka (Slovakia) is dated to the first half of the 6th millennium cal BC, making it the earliest pottery north of the Danube. It seems feasible that ceramic containers from Santovka were produced by hunter-gatherers, and pottery predated the arrival of farming in the Carpathian region by a couple of centuries.

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ABSTRACTWe present two new millennium-long tree-ring oxygen isotope chronologies for central and northern Japan, based on 9693 annually resolved measurements of tree-ring oxygen isotopes from 39 unearthed samples consisting mainly of Japanese cedar (Cryptomeria japonica). These chronologies were developed through cross-dating of tree-ring widths and δ18O data from multiple samples covering the periods 2349–1009 BCE (1341 yr) and 1412–466 BCE (947 yr) for central and northern Japan, respectively. In combination with our published chronology for central Japan, the tree-ring δ18O dataset currently available covers the past 4354 yr (2349 BCE to 2005 CE), which represents the longest annually resolved tree-ring δ18O dataset for Asia. Furthermore, the high-resolution temporal record of 14C contents independently developed by Sakurai et al. (2020) was reproduced by our 14C measurements of earlywood and latewood in annual rings for the period 667–660 BCE.

ABSTRACTThe lack of systematic chronologies is a key problem for the archaeological sites of Altai and adjacent territories during the Great Migration Period. Here we present an attempt to establish the chronology of the Bulan-Koby culture objects of the Karban-I necropolis by correlation of accelerator mass spectrometry radiocarbon (AMS 14C) data from human remains with data from archaeological dating methods. This is the first application of such a combined targeted 14C and archaeological approach to the chronology of the Great Migration Period materials of northern Altai, and in particular the Bulan-Koby culture. Systematic analysis of the mutual occurrence of dated types of certain grave goods and 14C dating of a series of samples supports a predominant period of use for the site that spans the 2nd–3rd c. AD, which corresponds to the early Xianbei period. This study demonstrates strong agreement between the indicators obtained by archaeological and radiocarbon methods, suggesting chronological consistency of the necropolis which functioned at the beginning of the Great Migration Period. The very combination of the two techniques will allow more precise and detailed chronologies for other archaeological complexes of Altai and adjacent territories from the first centuries of the 1st mil. AD, which is the basis of historical reconstructions.