- Research Article
- 10.2118/233367-pa
Upscaling Characterization of Mechanical Properties of Shale Based on the Constrained Big Data Nanoindentation
- Mar 01, 2026
- SPE Journal
- Min Zhang + 4 more +4
Summary The characterization of ultradeep shale reservoirs is hindered by the scarcity and limited size of available samples. With this study, we develop a constrained big data nanoindentation analytics framework for the upscaling characterization of shales, integrating mineralogical and microstructural constraints into grid-based nanoindentation data sets. The three dominant shale minerals are further classified into five representative microstructural types based on their distinct microscopic mechanical responses. Significant variations in elastic modulus and fracture toughness are observed among microstructures of the same mineral composition. Compared with conventional composition-based upscaling, the microstructure-constrained model yields results that are in closer agreement with macroscopic laboratory measurements. The error between the upscaling modulus and the static elastic modulus under 30-MPa confining pressure does not exceed 5.38% when indentation depth exceeds 350 nm. The homogenized modulus from the surround effect model differs by merely 2.1% from the dynamic modulus derived from P-wave velocity. Microcrack accumulation around mineral debris clusters (MDCs) is identified as the dominant mechanism controlling fracture propagation in three-point bending (TPB) tests. Moreover, the microscale fracture toughness of MDCs obtained from nanoindentation agrees well with the effective fracture toughness estimated from the upscaling size effect model. These findings establish an upscaling method for ultradeep shale reservoirs and provide a mechanistic basis for optimizing hydraulic fracturing design and shale gas production efficiency.
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