ABSTRACTThe origin of Ireland’s fauna is an unresolved issue in the history of the island. Although researchers once considered Ireland’s mammals to have spread to Ireland during the early postglacial from 11,700 cal BP, research has increasingly suggested humans translocated many of these species to Ireland. However, due to sparse evidence, the origin of Ireland’s purported native mustelid species remains unanswered. In this study, we shed light on the history of otter and badger in Ireland by directly dating suspected early examples of these species from Derragh, Co. Longford, a late Mesolithic campsite. The results demonstrate that both of these species have been present in Ireland for at least 7000–8000 years. It is not clear if they represent self-colonisers or Mesolithic anthropogenic translocations. Although these finds do not rule out local extinction and later reintroduction, they show that we can no longer assume they are solely late Holocene introductions.

ABSTRACT This research is performed on a selection of archaeological glass finds with corresponding soil samples, excavated on the site of the High Medieval castle Cucagna in Friuli/Northern Italy. In the frame of understanding medieval glass technology and the chemical–physical conditions that influenced the state of preservation of the glass finds, this study uses a multi-analytical line-up of methods to characterize the composition of the glass and basic parameters of the soil including texture, mineralogical composition, pH, redox potential (Eh) and electric conductivity (EC). The results show that glass corrosion in soil not only depends on acidity, alkalinity or glass composition but also on the texture of the soil, measurable as grain-size distribution, and the mineralogical composition. The compositional groups of the glassware from Cucagna indicate the use of various raw material sources, pointing to Northern and Central Italian glass workshops with primary or secondary glass production.

ABSTRACT Excavated glass artifacts are usually environmentally impacted, causing spatial inhomogeneity which poses great challenges for accurate and non-destructive chemical characterization. Here, we present our study on accurate characterization of archaeological glass with Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS), a high-precision and minimally destructive analytic method. Using three corroded glass beads excavated from Guangnan, Yunnan, Southern China as examples, we discuss the issues that may be involved when observing signal curves of highly inhomogeneous archaeological glass, as well as provide chemical characterization for the intact pristine body. Results indicate that these Indo-Pacific monochrome beads are of the potassium silicate glass type and used mineral potash source, and that they contain copper as the colorant. By discussing the breadth and depth types of inhomogeneity and focusing on perturbation endured by major elements, we identify the extent of environmental alteration and describe how different elements and matrices can respond differently to the archaeological environment, leading to various corrosion behaviors. For such samples LA-ICP-MS is shown to be an advantageous tool to provide archaeologically relevant information, or to probe artifact conditions for conservation purposes. A good understanding of sample conditions, and close attention to the experimental and calibration process are required to overcome inhomogeneity when tackling archaeological glass.

ABSTRACT Cobalt was commonly used as a colourant in the Egyptian glass industries of the 18th dynasty, dark blue glass being a regular find at palatial and settlement sites, including Amarna and Malqata. The main source of cobalt ore used during this period has been identified in the Egyptian western desert, around the oases of Kharga and Dakhla. In order to better understand the chaîne opératoire of Late Bronze Age glass production and -working, in particular with regard to cobalt ore, at Amarna, chemical analysis by portable X-Ray fluorescence was carried out in the field. This was done on contextualised archaeological material excavated at the site of Amarna, which cannot be exported from Egypt for analysis. The results of this study demonstrate how cobalt ore was used in the various known workshop sites at Amarna, resulting in a deeper understanding of raw materials use and exchange across this settlement.

ABSTRACTThis paper proposed phytoliths as promising for identifying and distinguishing sources of fibre in Chinese handmade papers. For an initial methodological exploration, two types of Raw Xuan (unprocessed Xuan paper) and the two plant materials used in making them—namely rice straw and bark from blue sandalwood (Pteroceltis tatarinowii Maxim.)—were collected. The dry ashing method was used to extract phytoliths from Raw Xuan and its plant materials.The results can be summarized as follows. First, phytoliths characteristic of rice (Oryza sativa) were abundant in both rice straw and Raw Xuan. By looking for rice phytoliths, it is possible to tell whether or not rice straw fibre is used in a particular paper. Second, hair cell phytoliths were observed in considerable quantities in blue sandalwood bark, but absent in the examined papers. Heat experiments showed that phytoliths in blue sandalwood were resistant to long-term heat and they would unlikely be eliminated when exposed to the heat in papermaking (with heat source barely above 200°C). It is hypothesised that they dissolved while cooked in an alkaline pH (limewater). Further studies are necessary to understand whether phytoliths in blue sandalwood—while cooked in limewater—undergo morphological changes and, if yes, how.

ABSTRACTDuring the 2nd millennium BC anthropomorphic menhirs belonging to a 3rd millennium BC sanctuary were reused as building material in the Arasseda Nuraghe (Sardinia, Italy). To analyse the Arasseda menhirs and the local Monte Ironi geological samples (presenting similar visual features), chemical (pXRF, ICP-OES, ICP-MS), mineralogical-chemical (PXRD) and physical (Mohs hardness) measurements were performed. Through the experimental data, the menhirs source provenance and the technological properties (workability, durability) of the raw material chosen for sculptural purposes during Copper Age were investigated. To the authors’ knowledge this is the first archaeometric study on the Arasseda menhirs (the third on Sardinian menhirs) and one between the few recently developed on European megaliths.

ABSTRACTThe Digital Helike Project aims at the digitization of archaeological data from the Helike Project, Achaia, Greece. This paper advances understanding of Early Bronze Age house building techniques with focus on corridor houses. The Helike Corridor House is a fine example of an architectural style of the Early Helladic period EH II/Early EH III on the Greek mainland and it is used here as a case study. A methodology for 3D reconstruction is described supporting both structural integrity simulations and advanced visualization studies. The paper focuses on three aspects: firstly, it highlights technological innovations in the Bronze Age period by drawing attention to structural integrity studies recently carried out by the research team; secondly, it describes a methodology for building fully geo-referenced 3D models supporting structural integrity studies and visualization on GIS-Geographic Information Systems; and thirdly, it leads to the universal access of data and visualization over the Internet through the selection of appropriate open source, open standards and freely available tools and applications. The methodologies proposed here deepen insights on archaeological data enabling new inferences and knowledge to be gained through the implementation of universally shared low cost applications.

ABSTRACTNon-destructive prompt gamma activation analysis (PGAA), neutron radiography (NR) and high resolution time-of-flight neutron diffraction (TOF-ND) have been applied to investigate metal archaeological artefacts belonging to the Academia Georgica Treiensis (AGT) collection. 8 archaeological items have been analysed, by using the facilities of the Budapest Neutron Centre (BNC). Some of these objects mostly dating back probably to the VI-IV century B.C. and presumed to be discovered in the Marche Region, Italy. The primary goal of the analyses was to advance the correct technological and material description of the objects, providing scientific data for further and more comprehensive comparative analyses also covering the find material from the close archaeological sites.The neutron investigations allowed determining the bulk composition, also providing either a qualitative and quantitative assessment of the phase composition and the structural properties of the constituents, or radiographic images, which would finally help to identify possible manufacturing techniques.Additional examinations, carried out by external milli-beam particle induced X-ray emission spectroscopy (PIXE), provided quantitative analyses of major and trace elements (e.g., Fe, Pb and As) in order to recognize the constitutive alloys and to supply information on the near-surface elemental composition, complementary to the data characteristic for the bulk.The obtained results, thought to be useful to set up a classification according to the chemical composition, and this way allow achieving important information related to the possible provenance of the objects.

The historical framework for the discussion is the chronology of Sri Lankan culture, which, based on the most recent archaeological evidence and radiocarbon dates, has been defined by three major periods: Early Historic (500 BC-300 AD), Middle Historic (300 AD-1200 AD) and Late Historic (1200 AD-1815 AD). A classification for the evolution of bronze sculpture with reference to the established historical chronology for Sri Lanka has been proposed by Reedy (2007) who sets out the following four major developmental periods of Late Anuradhapura (ca.432–993 AD), Polonnaruva (late 10th to early 13th century), Divided Kingdoms (13th to late 16th century), and Kandyan (17th to 19th century). This technical study investigated thirty sculptures including 25 tin bronzes in The Metropolitan Museum of Art and five from the Archaeological Department of Sri Lanka, representing all four major historic periods. The methods used to analyse the manufacture, composition, and condition of the statues were examination under magnification and Ultraviolet light, X-ray radiography, elemental analysis using X-ray fluorescence spectroscopy, and metallography. The results of the study included the finding that all the statues in the sample were cast using the lost-wax technique. Size does not seem to have had a bearing on whether statues were cast solid or hollow. Many of the small seated figures in the sample were solid cast, while a few were hollow cast. In addition the radiographs indicate that a variety of armatures of different thickness, size, and shape were present inside the hollow figures, irrespective of the size of the statues. Generally, metal of low porosity and few casting defects are observed in most of the radiographs, indicating that the castings are generally of good quality. Traces of five gates (or vents) observed on the backs of a group of five Lokapala figures examined, indicated that they were cast face-down in a horizontal position. Ten figures, particularly those from the later periods, show traces of gilding or intact gold layers. In all but one case, gold was found in association with mercury, confirming that they were amalgam gilded. Metallurgical studies were carried out on four figures in the sample: a Buddha, a Bodhisattva and two Hindu deities. A sample from a tang that was cast onto the goddess figure in antiquity proved to be quenched high-tin bronze, as evident from its microstructure; a tin content of 24.8 w/o was confirmed using X-ray energy dispersive spectroscopy in a scanning electron microscope. The four statues were from different historical periods and showed different microstructures, reflecting dissimilarities in composition, thermal history, and state of preservation.

The first results of textile and dye analyses of cloth remains recovered in Samdzong, Upper Mustang, Nepal, are presented. The site consists of ten shaft tombs, dated between the 400-650 CE, cut into a high cliff face at an elevation of 4000 m asl. The dry climate and high altitude favoured the exceptional preservation of organic materials. One of the objects recovered from the elite Samdzong 5 tomb complex is composed of wool fabrics to which copper, glass and cloth beads are attached and probably constitutes the remains of a complex decorative headwear, which may have been attached to a gold/silver mask. SEM was used to identify the fibre sources of the textiles, which are all of animal nature. Two of the textiles are made of degummed silk. There is no evidence for local silk production suggesting that Samdzong was inserted into the long-distance trade network of the Silk Road. HPLC-DAD analysis permitted identification of a variety of organic dyes, including Indian lac, munjeet, turmeric and knotweed/indigo, while cinnabar was identified through micro Raman spectrometry. The results indicate that locally produced materials were used in combination with those likely imported from afar, including China and India.Statement of significance Textiles are not commonly found in most archaeological contexts, yet when preserved in organic state they can be analysed using modern scientific techniques such as Scanning Electron Microscopy and High Performance Liquid Chromatography to uncover information about their fibre and dye sources. This information can be used to reconstruct the economic and social aspects of textile production and exchange in the past. Identification of silk fibres and munjeet and Indian lac dyes in the textile finds from Samdzong, Nepal suggests that imported materials were used in combination with those locally produced.Data availability The authors confirm that all data underlying the findings are fully available without restriction. All relevant data are contained within the paper.