3D memory chip stacking by multi-layer self-assembly technology

As device-scaling challenges increase, three-dimensional (3D) integrated circuits (ICs) are receiving more attention for system performance enhancements, due to their higher interconnect densities and shorter interconnect lengths. However, because of the limited contact area and the higher circuit density, the cooling of 3D ICs is more challenging. In order to assess appropriate cooling solutions for 3D chip stacks in various uses, we need better understanding of the total thermal resistance of 3D chip stacks. This calls for precise thermal resistance measurements and thermal modeling for each component of a 3D chip stack. A 3D chip stack is composed of interconnections, silicon substrates, back-end-of-the-line (BEOL), front-end-of-the-line (FEOL) and in this study, the thermal resistance of interconnections is the primary focus because interconnections are regarded as one of the thermal resistance bottlenecks of a 3D chip stack. With regard to the thermal resistance measurements of interconnections, Yamaji et al. found it difficult to measure the thermal resistance of interconnections with the laser-flash method and pointed out that care was necessary for uniform temperature distribution in the sample when using the laser-flash method on heterogeneous specimens, such as stacked chips with interconnections. Considering this concern, we use a steady-state method for the thermal resistance measurements of the interconnections. The thermal resistance of 200μpitch-C4 (Pb97Sn3) joined samples is measured and the thermal conductivity of C4 is derived to be 18 – 24 W/mC. Also the thermal resistance of a silicon with various interconnection pitches and diameters is modeled and the relationship of thermal resistance to interconnection pitch and diameter is obtained. The thermal resistance reduction by underfill with various interconnection pitches and diameters is also studied.

In order to determine appropriate cooling solutions for 3D chip stacks in various cases, it is important to have a better understanding of the total thermal resistance of a 3D chip stack. For this purpose, precise thermal resistance measurements and modeling of each component of a 3D chip stack are important. The thermal resistance of interconnection is considered to be one of the thermal resistance bottlenecks of a 3D chip stack. In this study, a steady-state thermal resistance measurement method is employed for the thermal resistance measurement of interconnection. The thermal resistance of the 200 μm pitch C4's (Pb97Sn3) jointed samples are measured and the thermal conductivity of C4's is derived to be 18–24 W/mK. With regard to the thermal resistance of a silicon substrate, the thermal resistance of a silicon substrate with various interconnection pitches and diameters has already been modeled by considering the concentrated heat flow to interconnection, as presented in ICEP 2008.[15] Based on the modeled data, the thermal resistance reduction by underfill with various interconnection pitches and diameters is also studied.

For the thermal management of three-dimensional (3D) chip stack, its thermal resistance needs to be clearly understood. In this study, 3D stacked test chips are fabricated, which are implemented with PN junction diodes for temperature sensors and diffused resistors for heating. At SemiTherm2011, the equivalent thermal conductivity of the interconnection, including BEOL (Back-End-Of-the-Line, wiring layer) is experimentally obtained to be 1.6W/mC and this time, we measure the thermal effect of Cu TSVs and it is experimentally supported that as the Cu TSV area ratio increases, the thermal conductivity of chip with TSVs in the vertical direction increases, on the contrary, that in the horizontal direction decreases. Also, the transient thermal measurement is performed and its result is compared with steady state measurement result. Further, the thermal capacitance measurement of 3D stacked test chip with hot spot heating is performed, which is essential to determine the transient thermal performance of 3D chip stack.

In order to achieve the shorter circuit design of multiple chips, three-dimensional (3D) packaging technologies with through silicon vias were developed to achieve high performance, low power consumption and small packaging size. In this paper, a PCB (Printed Circuit Board) processing compatible structure of three-dimensional chip stacking with low cost and easy fabrication will be shown. 3D and through Si via connections were formed by UV laser drilling technology. Laser drilling is a non-contact manufacture method and laser beam with high energy can be focused to a small spot (15 mum beam diameter) for material ablating and removing without mask used. Several processes are the keys to accomplish 3D stacking, such as wafer thinning process, through silicon via forming process, dielectric layer forming process, metallization process, and inter chips bonding process. By integration of the mentioned key processes, a 3D chip stacking structure with 10 layers was carried out. The thickness of chip was 100 mum. Daisy chain pattern was designed for the electrical measurement of 3D stacking structure. The testing results show that the resistance of multi- chip stacking structure is about 0.056 Omega/cm. Some reliability test, such as temperature cycling test and pressure cooker test were also done. These testing results verified this PCB processing compatible 3D chip stacking technology with low cost is a reliable structure for 3D SiP (System in Packaging) module application.

Cooling of a planar 2D IC chip utilizes heat transfer from a face of the chip though a heat sink. In case of a 3D IC chip stack, the individual chip faces are not available for mounting conventional heat sinks. Mounting the heat sinks on the ends is feasible, but the heat flow paths for the interior chips from the junction to the heat sink become longer. Further, multiple heat sources present along the heat flow paths in stacked chips may create localized hot spots which exceed the allowable junction temperatures. While 2.5D integration in complex ICs where individual layers are mounted on another base die called an interposer can alleviate the heat dissipation issues, it cannot deliver the benefits of monolithic 3D ICs due to the planar distance between the chips or chiplets over the interposer. Introducing interlayer cooling with microchannels and introducing fins in the coolant flow paths extend the thermal dissipation capability of a 3D stack; however this is often accompanied with taller microchannels that lead to longer lengths of through-silicon-vias (TSVs). Placement of TSVs, microchannels walls and fins present conflicting design requirements. Therefore co-design and innovative approaches are seen as critical before widespread commercialization of 3D ICs becomes a reality. An overview of the available cooling options for 3D ICs and their performance evaluation are presented in this chapter.

With the increased demand of functionality in electronic device, three dimensional integration circuits technology together with downscaling of interconnection pitch present an important role for the development of next generation electronics. In the current types of interconnects, solder micro bumps have received much attention due to its low cost in material and process. For fine pitch solder micro bump interconnections, selection of under bump metallurgical material is a crucial issue because the UBM structure/material will show a significant influence on the reliability performances of the solder micro bump joints. However, which UBM structure/material for fine pitch solder micro bump joint presents the better reliability properties is not concluded yet until now. In this study, the effect of UBM structural/material on the reliability properties of lead-free solder micro interconnections with a pitch of 30μm was discussed. The chip-on-chip test vehicle with solder micro bump interconnections having a diameter of 18 μm was adopted to evaluate the effects of UBM structure/material. There were more than 3000 micro bumps with Sn2.5Ag solder material on both the silicon chip and carrier. In this study, three types of UBM were selected on the silicon carrier: they were single copper layer with a thickness of 8μm; the Cu/Ni layer with the thickness of 5μm/3μm and the Cu/Ni/Au layer with the thickness of 5μm/3μm/0.5μm. The UBM was electro-plated on the Al trace and then the Sn2.5Ag solder with a thickness of 5 μm was deposited. For the silicon carrier with the bump structure of Cu/Sn and Cu/Ni/Sn, the silicon test chip with solder micro bump of Cu/Sn was used for chip bonding. The test chip having the solder micro bump of Cu/Sn and Cu//Ni/Sn was used for bonding with the silicon carrier having the Cu/Ni/Au UBM. In chip stacking process, we adopted the fluxless thermocompression process for each type of micro joints. After chip bonding process, the fine gap between bonded chips was filled by capillary type of underfill. The influence of underfill on the reliability of solder micro bump interconnects with various combinations of UBM structures were estimated also. After the assembly process, temperature cycling test (TCT), high temperature storage (HTS) and electromigration test (EM) were performed on the chip-stacking module to assess the effect of UBM structure/material on the reliability of solder micro bump interconnections. The results of reliability test revealed that only Cu/Sn/Au/Ni/Cu micro joint could not pass the TCT and HTS of 1000 cycles. After reliability test, the Cu/Sn/Cu joints showed the evidently microstructural evolution while the Cu/Ni/Sn/Cu joints did not show apparent microstructure change among all the types of micro joints and still revealed the most contents of residual solder within the joint. On the other hand, the existence of Au layer upon the UBM caused the complicated interface reaction between solder and UBM, which presented a negative effect during long-term reliability performance. The reliability results also displayed that the introduction of underfill could apparently enhance the reliability of micro joint under mechanical evaluation. From the results of EM reliability test, all the types of the micro joints showed excellent electromigration resistance under current stress of 0.08A at an ambient temperature of 150°C irrespective of the types of UBM. This superior property was attributed to the microstructure change transformed from the solder joint to the IMC joint within the solder micro bump interconnections during electromigration test. All the results of reliability test illustrated that the selection of UBM structure/material well influenced the reliability performance of fine-pitch solder micro bump interconnections in 3D chip stacking.

As the demands of functionality and performance for electronic products increase, three-dimensional chip stacking with high-density I/O has received much attention. For high density interconnections packaging, solder micro bumps are adopted extensively. However, its process temperature is high during chip stacking process. High bonding temperature would be easy to lead chip damage and chip warpage. For diminishing the thermal damage resulted from the high bonding temperature during chip stacking, we used the anisotropic conductive film as an intermediate layer to bond the chips. In this paper, a new type of ACF with Ni/Au-coated polymer arrayed particles was adopted for assembling a chip stack module with a micro bump pitch of 30μm. The reliability of the chip stack assembled by such novel material was evaluated and estimated also. The chip-to-chip stack module having more than 3000 I/Os with a pitch of 30μm was used as the test vehicle. The structure of Cu/Ni/Au micro bump was chosen and fabricated on both the silicon chip and substrate. The silicon chip was bonded onto the silicon substrate using the arrayed-particles ACF material after ACF lamination process. The optimized lamination conditions and the effects of bonding pressure and temperature were evaluated and determined by considering the particle deformation, electrical performance and adhesive flow phenomenon. After optimizing the lamination and bonding parameters, the reliability of the assembled C2C module was evaluated by Pre-condition test, TCT and THST. Cross-sectioned inspection of micro joints by scanning electron microscopy, observation of interface between adhesive and silicon by scanning acoustic tomography, and adhesion test of ACF film after bonding and precondition were conducted to determine the failure modes of the ACF joining. After precondition test, less than 15% of daisy-chain resistance variation was found. The ACF joints with stable electrical resistance could be obtained by such kind of novel material. Also, no any obvious ACF delamination could be observed. The adhesion strength did not show any degradation after precondition test. The reliability test results revealed that the assembled C2C module by the arrayed-particles ACF showed the acceptable reliability performance in TCT and THST. The results of failure analysis displayed that the connectivity of ACF joints was damaged by induced thermal stress coming from the mismatch of CTE between adhesive matrix and conductive particles during environmental testing. This study presented that the arrayed-particles anisotropic conductive film adopted had great potential and could be applied for the 3D chip stacking assembly with fine pitch interconnects.

Three-dimensional (3D) integration technology promises to continue enhancing integrated-circuit system performance with high bandwidth, low latency, low power, and a small form factor for a variety of applications. In this work, conventional C4 (controlled-collapse chip connection) technology is studied for robust interconnection between stacked thin chips. Various solder hierarchies to enable 3D chip stacking and packaging are investigated. Examples are presented to compare stacking schemes with sequential and parallel reflow. Chips as thin as 90 µm are stacked using conventional chip-placement and reflow processes, and the associated process challenges are investigated and discussed. Warpage of the thin chips is measured on various substrates. Rework of the chip stack has also been demonstrated through a temporary chip attachment operation, and the scalability of reworkable C4 is investigated.

Three dimensional (3D) integration technology, involving the vertical stacking of multiple chips using through-silicon vias (TSVs), has emerged as a promising solution to improve the performance of microelectronic devices. However, the complex structures and the consequent increase in power density exacerbate the challenge of thermal management in the device including multiple chips. In order to ensure the reliability of 3D stacked chips during operation, it is important to have a better understanding of the thermal distribution of a 3D chip stack. In this paper, a detailed analysis of 3D IC packaging from thermal reliability perspective is presented, performed by finite element simulations. The effect of the variation of structure-related parameters on steady-state temperature profiles in the stack has been analyzed, including TSVs diameter and pitch, the thickness of SiO 2 , as well as the thermal conductivity of under fill. The research provides useful insights for thermal management of 3D IC packaging.

3D stacking of dies is a promising technique to allow miniaturization and performance enhancement of electronic systems. The complexity of the interconnection structures, combined with the reduced thermal spreading in the thinned dies and the poorly thermally conductive adhesives complicate the thermal behaviour of a stacked die structure. The same dissipation will lead to higher temperatures and a more pronounced temperature peak in a stacked die package compared to a single die package. Therefore, the thermal behaviour in a 3D-IC needs to be studied thoroughly. In this paper, a test vehicle to assess power dissipation in multiple hot spots and the thermal impact of TSVs, is presented. In this test vehicle, a stack of test chips with integrated heaters and temperature sensors is used to evaluate the steady state and transient temperature profile of multiple hot spots. With this experimental set-up, the thermal modelling of the 3D stacks is validated.

Increasing demand for new and more advanced electronic products, with smaller form factor and superior functionality and performance, while reducing the cost, has driven the semiconductor industry to develop more innovative and emerging advanced packaging technologies. 3D packaging, using z-axis through silicon via (TSV) stacking concept has been and continues to be investigated by many of the semiconductor manufacturers and research institutes and is believed to be one of the most promising, if not the most promising concept that could successfully address the limitations of today's packaging technologies. There is a continuous increase of interest in development and study of applicability of this new chip stacking approach to existing and future devices; currently, more than fifty companies worldwide are involved in some sort of 3D TSV packaging developments. There are several steps involved in 3D chip stacking using TSV technology. Each of these steps requires different techniques, materials and processes, applications that have to be well understood and integrated in order to successfully be applied. This paper will address various electrodeposition processes applied to form 3D interconnects, from TSV deposition, which is the main metallization step that stays at the hearth of this new technology, to other metallization steps for additional connections, such as bumping and redistribution layers, already well known and applied processes in current wafer level packaging (WLP) applications. Advantages and difficulties associated with each of these technologies, with more focus on 3D vertical integration using TSV copper interconnect, including the approaches taken to overcome them, will be presented. Deposition conditions for bumping were optimized in order to enable higher deposition rates. For other through- mask applications, such as redistribution lines (RDL), the complexity of the pattern, deposition rate, chemical formulation and process parameters were found to have a significant effect on within-die (WID) thickness distribution. In case of WLP structures of thick metal and high aspect ratios, seed layer uniformity proved to be essential for achieving void-free deposition. Void-free structures, especially for high aspect ratio vias seeded with dry methods, such as physical vapor deposition (PVD) or chemical vapor deposition (CVD), seem difficult to obtain. New approaches, such as seed layer repair (SLE) or direct on barrier electrodeposition (DOB) can provide superior uniformity and coverage of the conductive layer, necessary for a uniform nucleation of copper electrodeposition process along the entire sidewall of the via, at significantly lower costs. This paper will present TSV structures obtained with wet chemical processes applications for both seed layer and via filling. Besides seed layer uniformity, additional factors were identified to also be critical for successfully filling deep vias. They are: via profile, wettability of vias, superior performance of chemistries and high performance equipment. By selecting the most appropriate deposition methods and optimizing the chemical formulations together with the process parameters, void-free TSV structures can be obtained.

3D chip stacking with through silicon vias (TSVs) has been identified as one of the major technologies for achieving higher silicon packaging density and shorter interconnect. The test vehicle presented in this paper is a 3D chip stack package. Each layer of the test vehicle has two silicon flip chips mounted at the bottom of a silicon interposer with solder bumps. The flip chip has the equivalent dimensions and pad patterns as commercial memory chips. The interposer, with multiple interconnect TSVs for electrical connection and a central TSV for underfill dispensing, can function as a logic chip or as a redistribution chip in a real application. The assembly steps of the test vehicle include conductive adhesive filling for the interconnect TSVs, bonding two bumped flip chips on an interposer (to form a single layer), vertical stacking of the single layers and underfill dispensing. For the filling of the interconnect TSVs, an auger-dispensing method is first adopted to overfill the interconnect TSVs, followed by removing the excessive adhesive beyond the interconnect TSVs by squeegeeing. A jet valve continuously dispenses free dots of an underfill encapsulant into the central TSVs. The central TSVs function as an entrance for underfill dispensing and an uninterrupted point-source to provide fluid for each layer. The free dots form a capillary flow to fill the under-chip spaces of the test vehicle. The usage of TSVs rather than chip edges eliminates the presence of a wide edge reservoir, resulting in smaller ‘keep-out’ area occupation on the substrate.

HotSpot is an open source analysis tool for estimating temperature of both 2D and 3D chip stacks. It counts both the primary path of the heat transfer through the heat-sink and the secondary path through the print circuit board. It can estimate the temperature of chips. However, HotSpot-6.0 cannot treat a complicated chip stacking such as the castle of chips (CoC) with inductive wireless coupling through-chip interface (TCI). Therefore, in this report we have extended the HotSpot simulator and updated it in order to evaluate CoC. Compared to the original HotSpot, the extended version of HotSpot had an average execution time increase of about 6% when evaluating the same vertical stacking. The execution time of CoC with the same number of chips is shorter than when executing vertical stacking, but when the number of layers is the same, the execution time is almost equal. Moreover, our design considers high productivity, e.g. it can easily set air cooling, oil cooling, water cooling evaluation and chip rotation setting.

The rapid increase in on-chip heat fluxes and package heat density, accompanying the migration to nanoelectronics and 3D chip stacks, has placed thermal management squarely on the critical path for advanced product development. Innovative, cost-effective cooling techniques, combined in a synergetic way with more conventional approaches, must be developed if the benefits of the Moore's Law progression are to be realized. Following a brief discussion of the industry roadmap for IC packaging and review of chip package thermal management options, attention will turn to the application of solidstate thermoelectric refrigeration and the thermal characteristics of direct immersion cooling in dielectric liquids. The presentation will close with a discussion of the research challenges associated with the commercial implementation of on-chip thermoelectric coolers and direct liquid cooling.

Requirements of a quantum beam imager such as a vertex detector in high energy physics experiment are intelligent functions which are realized by embedding memories of quantum beam hit-position, hit-charge, and hit-timing in a pixel with keeping small pixel size to achieve high spatial resolution. To satisfy the requirements, circuit layer stacking on a sensor, i.e., three dimensional (3D) technology, has been widely studied and proposed. The Silicon-on-Insulator (SOI) sensor is one of the 3D sensors because the circuits in the top silicon layer is on the sensors of the bottom silicon substrate. The circuits and sensors are electrically connected by submicron W filled vias through the buried oxide (BOX), which are called as through BOX vias (TBV). Thus, the SOI sensor has extremely higher fill factor than the bulk-CMOS sensor. In order to achieve more intelligent functions in the pixel, however, the pixel size by using the simple SOI technology is large to get the required spatial resolution. Therefore, multiple circuit layer formation by chip stacking technology is adopted. In this chip stacking, a fine pitch micro-bump technology with two-tile face-to-face stacking is employed because of the simplest 3D structure. The target of micro bump diameter and spacing are 2.5 μm and 5 μm, respectively. The SOI 3D chip stacking process is starting with the base chips which are fabricated by an 8 inch 0.2 μm fully depleted SOI pixel sensor process with five metal layers. After the metal 5 etching, an oxide film is deposited and planarized by chemical mechanical polishing (CMP). W-filled vias to a under bump metal is formed at bump formation areas. After the under bump metal deposition and patterning, metal bumps are formed. Then, two chips which are lower and upper chips are aligned and bonded face-to-face at 200℃ followed by adhesive injection. To make bonding pads on the upper chip, the upper chip handle silicon is etched until exposing the BOX and TBV by wet solution. TBV can easily connect between circuits in the upper chip and the bonding pad metal without any through silicon via (TSV) process. This is the most superior point to use the FD-SOI pixel sensor in 3D structure. The TBV size is around 0.3 μm which is much smaller than a conventional TSV whose size is around 5 μm by using the most advanced technology. In addition, this TBV can be used as interconnections between multiple chips without any TSV. Finally, bonding pad and passivation formation are done. For micro bump formation, a gold bump was utilized because the gold is oxidation-resistant metal. The micro gold bump was fabricated by two methods. One is a cone shaped gold bump manufactured by a gold nanoparticle deposition with a photoresist lift-off technique [1]. The cone shaped gold bump with 2.5 μm in diameter and 2.5 μm in height are successfully formed on the under bump metal layer. Because of the nanoparticle deposition, the gold bump is easier to deform by the bonding. Thus, the collapsibility allows low stress to the die and high reliable junctions. It is also confirmed that the bump resistance is approximately 0.25 Ω/bump from daisy chain measurement. The other is a gold cylindrical bump using a combination of inverse-tapered photoresist and low incident angle sputtering [2]. Because of narrowing at the top, lower pressure to collapse between the bumps is required than the gold cone bumps. This may also improve bump yield and reliability. 0.37 Ω/bump of the bump resistance is obtained by the gold cylindrical bumps. Using the FD-SOI 3D chip stacking technology with the cylindrical bump, the pixel sensor designed for the International Linear Collider (ILC) vertex detector called SOFIST was fabricated and the chip photo is shown in the figure. In SOFIST, hit-position, hit-charge, and hit-time memories are embedded in each pixel by the 3D micro bump bonding with 20 mm pixel size. Owing to the removal of the handle silicon of the upper chip, the patterns of the lower chip can be seen through the upper chip oxide. The green patterns close to bonding pads are backsides of silicon layer in the upper chip. As shown in the figure, our 3D process technology is successfully introduced in FD-SOI quantum beam imager.